Commit c01391de authored by Jan Zelenka's avatar Jan Zelenka
Browse files

Readme - minor fixes

parent 81e2d754
......@@ -2,24 +2,23 @@
If you are new to ISQ and need access to it, please read the following guide.
### How to operate the machine
I've made a video. Its not perfect, but most of the things are covered. Bottlenecks of this video-guide are listed below. Once stable operation procedure will be developed fixed video will be recorded.
I've made a video. Its not perfect, but most of the things are covered. Bottlenecks of this video-guide are listed below. Once stable operation procedure will be developed, fixed video will be recorded.
#### Video (youtube)
[![IMAGE ALT TEXT](http://img.youtube.com/vi/M8Ol5ormuOg/0.jpg)](http://www.youtube.com/watch?v=M8Ol5ormuOg "ISQ operation guide")
#### Notes (FAQ)
* PAY SPECIAL ATTENTION !! DO NOT SET BLANK AS TYPE:BLANK, keep the type as UNKNOWN.
* Sample tray is not fully visible in the video, check the photo inset.
* PAY SPECIAL ATTENTION !! DO NOT SET BLANK AS TYPE:BLANK, keep the type as UNKNOWN (as shown in the video).
* Sample tray is dispayed in the video in the photo inset.
* Sample tray can be moved by hand when not injecting.
* Mass-range is predefined to full operational range
* keep attention to setting proper method - correct solvent and correct mode (positive/negative)
* Stay away of pollutants!!
### How to gain access
Once MS tutors will be set the procedure should be easy.
* Contact your MS tutor.
* Watch the video.
* Measure few samples with the MS tutor.
* Measure few times with the MS tutor.
* Request MS tutor to write me (Jan) and I will grant you access for the booking system.
### Booking system
......@@ -27,7 +26,7 @@ Once MS tutors will be set the procedure should be easy.
### Known Pollutants
* polar aprotic solvents (DMF, DMSO, HMPA..)
* buffers (TEAB ..), concentrated ionic/easily ionizable compounds (TEA, DIPEA..)
* buffers (TEAB ..) and concentrated ionic/easily ionizable compounds (TEA, DIPEA..)
* electrolytes (TBAF, TBAPF6, ...)
* molecular sieves, microcrystalline compounds
* low-grade solvents
......
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